dc.contributor.advisor | Jurisson, Silvia S. (Silvia Sabine) | eng |
dc.contributor.author | Junnotula, Sulochana | eng |
dc.date.issued | 2006 | eng |
dc.date.submitted | 2006 Fall | eng |
dc.description | The entire dissertation/thesis text is included in the research.pdf file; the official abstract appears in the short.pdf file (which also appears in the research.pdf); a non-technical general description, or public abstract, appears in the public.pdf file. | eng |
dc.description | Title from title screen of research.pdf file (viewed on August 24, 2007) | eng |
dc.description | Includes bibliographical references. | eng |
dc.description | Thesis (M.S.) University of Missouri-Columbia 2006. | eng |
dc.description | Dissertations, Academic -- University of Missouri--Columbia -- Chemistry. | eng |
dc.description.abstract | The main focus of this thesis is the synthesis and characterization of nonradioactive rhenium complexes containing O, N, S ligands. Chapter 2 describes the rhenium labeling of four somatostatin analogues. Confirmation for the formation of nonradioactive rhenium labeled peptides was accomplished with LC-MS. Purification was done by analytical HPLC. Chapter 3 describes the synthesis, characterization and determination of acid dissociation constant values for the two rhenium complexes with ethylenediamine type ligands. This chapter also describes the synthesis and characterization of a rhenium amine complex with the 2-aminoethanethiolate ligand and a phosphine ligand. | eng |
dc.identifier.merlin | b59445269 | eng |
dc.identifier.oclc | 166289778 | eng |
dc.identifier.uri | https://hdl.handle.net/10355/4515 | |
dc.identifier.uri | https://doi.org/10.32469/10355/4515 | eng |
dc.language | English | eng |
dc.publisher | University of Missouri--Columbia | eng |
dc.relation.ispartofcommunity | University of Missouri--Columbia. Graduate School. Theses and Dissertations | eng |
dc.subject.lcsh | Rhenium compounds -- Synthesis | eng |
dc.subject.lcsh | Ligands | eng |
dc.subject.lcsh | High performance liquid chromatography | eng |
dc.subject.lcsh | Ethylenediamine | eng |
dc.subject.lcsh | Oxygen | eng |
dc.subject.lcsh | Nitrogen | eng |
dc.subject.lcsh | Sulfur | eng |
dc.title | Rhenium complexes with O, N, S ligands | eng |
dc.type | Thesis | eng |
thesis.degree.discipline | Chemistry (MU) | eng |
thesis.degree.grantor | University of Missouri--Columbia | eng |
thesis.degree.level | Masters | eng |
thesis.degree.name | M.S. | eng |