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    • Graduate School - MU Theses and Dissertations (MU)
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    • Dissertations (MU)
    • 2008 Dissertations (MU)
    • 2008 MU dissertations - Freely available online
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    Copper (I) coordination networks synthesized with solid-solid reactions

    Bockhold, Steven
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    [PDF] research.pdf (7.295Mb)
    Date
    2008
    Format
    Thesis
    Metadata
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    Abstract
    The use of solid-solid reactions in the development of one-, two-, and three dimensional Cu(I) coordination networks are discussed. The solid-solid reactions were monitored by a variety of instrumental techniques to achieve a better picture of the solid-solid reaction mechanism. The crystalline reagents led to crystalline products with no amorphous phase. The nitrogen containing bridging ligands, 4,7-phenanthroline, 4,4'- dipyridyl, and trans-1,2-bis(4-pyridy1)ethylene in addition to 1,3-dithiane were used in the formation of these networks. The resultant crystalline compounds were compared to the solution-based products, showing that on average the same product was formed. Through the bridging ligands and a change in the coordinated solvent, the ultimate goal of showing how these solid-solid reactions could be expanded to cover a large array of reagents was accomplished.
    URI
    https://doi.org/10.32469/10355/5612
    https://hdl.handle.net/10355/5612
    Degree
    Ph. D.
    Thesis Department
    Chemistry (MU)
    Rights
    OpenAccess.
    This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivs 3.0 License.
    Collections
    • Chemistry electronic theses and dissertations (MU)
    • 2008 MU dissertations - Freely available online

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