Mechano-chemical synthesis and analysis of zinc and pyrogallol [4] arene complex under solvent-free and ambient conditions [abstract]

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Mechano-chemical synthesis and analysis of zinc and pyrogallol [4] arene complex under solvent-free and ambient conditions [abstract]

Please use this identifier to cite or link to this item: http://hdl.handle.net/10355/909

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Title: Mechano-chemical synthesis and analysis of zinc and pyrogallol [4] arene complex under solvent-free and ambient conditions [abstract]
Author: Tabi, Harry E.; Power, Nicholas P.
Contributor: University of Missouri-Columbia. Office of Undergraduate Research
Keywords: chemical synthesis
green chemistry
solvent free
mechanochemical
Date: 2006
Publisher: University of Missouri--Columbia. Office of Undergraduate Research
Abstract: Herein, we report a solvent-free approach for chemical synthesis which focuses on mechanochemically forming products from reactants under ambient conditions. With this protocol, several organo-metallic complexes or frameworks of zinc and pyrogallol[4]arenes were synthesized and analyzed with MALDI-TOF mass spectrometry combined with solid state carbon thirteen Nuclear Magnetic Resonance (13CNMR). This synthetic approach is in line with the synthetic methodology of green chemistry which focuses on eco-friendly chemical synthesis or synthetic routs.
URI: http://hdl.handle.net/10355/909

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